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Diffuse reflectance IR spectroscopy along with H 2 and CO adsorption measurements were applied to the study of 0. Reduction of the catalyst at K results in formation of supported metallic Pt particles in SMSI strong metal-support interaction state, as evidenced by the sharp decrease of Pt ability to chemisorb H, at room temperature as well as the significant lowering of thermal stability of linear Pt-CO complexes. This is a preview of subscription content, log in to check access.

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Find more information on the Altmetric Attention Score and how the score is calculated. Transmission electron microscopy indicates that these bimetallic nanocluster particles have definitely monodispersed size-distributions, with each particle containing both nickel and palladium atoms. The alloy structure has also been shown by X-ray diffraction and extended X-ray absorption fine-structure analysis. X-ray absorption near-edge spectroscopic and X-ray photoelectron spectroscopic data have confirmed that the nickel in the bimetallic nanoclusters is in the zero-valence state, as stabilized by the presence of Pd.

The catalytic activities are demonstrated to be dependent on the metal composition of the particles.

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